Ampoule Furnace — User Manual
PDF · 26.09.14
Document language: English
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Ampoule Furnace
Compact research thermal reactor with ampoules, insert crucibles and chucks configured for the reaction conditions
An ampoule-type research thermal reactor for small-sample materials synthesis and heat treatment. Its compact structure is designed with glovebox installation in mind and supports rapid heating and rotational heat treatment. Quartz or Inconel ampoules can be configured with alumina, zirconia or boron nitride (BN) insert crucibles to prevent unwanted internal reactions. Choose chucks for rotation, vacuum, rotation with gas supply or reaction-temperature checking to suit the experiment.
Confirm the applicable model, options and final specifications before ordering.
Features
- Small-sample processing: ampoule-based materials synthesis and heat-treatment research
- Compact structure designed with glovebox installation in mind
- Rapid and rotational heat treatment: maximum heating rate of 200 °C/min by model and rotation speed of 100 rpm
- Ampoule options: Ø12 mm or Ø22 mm internal diameter, with quartz or Inconel materials
- Insert crucibles: alumina, zirconia or boron nitride (BN) to prevent unwanted reactions inside the ampoule
- Application-specific chucks for rotation, vacuum, rotation with gas supply, or reaction-temperature checking
Specifications
| Temperature Resolution | 0.1 °C |
|---|---|
| Rotation Speed | 100 rpm |
| Ampoule Internal Diameter | Ø12 mm / Ø22 mm |
| Ampoule Material | Quartz / Inconel |
| Insert Crucible Material | Alumina / Zirconia / Boron nitride (BN) |
| Chuck Diameter | Ø14 mm / Ø25 mm |
| Chuck Configurations | Rotating / Vacuum / Rotating with gas supply / Reaction-temperature checking |
| Configuration Note | Applicable chucks and configurations differ by ampoule reactor type. |
Confirm the final model-specific specification and options before ordering.
Specifications by model
| Parameter | TLP1109-AFP | TLP1109-AFH |
|---|---|---|
| Temperature Range | RT + 20 ~ 800 °C | RT + 20 ~ 1,050 °C |
| Maximum Heating Rate | 200 °C/min | 200 °C/min |
| Maximum Cooling Rate | 40 °C/min (400–800 °C range) | 40 °C/min (400–800 °C range) |
| Uniform-temperature zone | 20 mm | 20 mm |
| Dimensions (W × D × H) | 210 × 125 × 180 mm | 260 × 220 × 200 mm |
| Power Consumption | 0.6 kW | 1 kW |
Applicable chucks, ampoules and insert crucibles depend on the reactor configuration. Confirm the required configuration when making an inquiry.
Options
- Rotating chuck: rotational ampoule heat treatment
- Vacuum chuck: configurations for reactions under vacuum
- Rotating chuck with gas supply: combines rotation and gas introduction
- Reaction-temperature checking chuck: a configuration for checking reaction temperature
- Chuck diameter, ampoule material and insert crucible configuration matched to the ampoule reactor
Applications
- Small-sample materials synthesis and heat-treatment research
- Ampoule heat treatment of all-solid-state battery materials
Manuals & technical documents
1 results
RESEARCH APPLICATIONS
Research Publications
Reference information to help you understand research applications of the equipment.
Impact of conducting agents on sulfide and halide electrolytes in disordered rocksalt cathode-based all-solid-state batteries
EcoMat · 2024
Equipment · model
Ampoule Furnace · TLP1109-AFH
Heat-treating halide electrolytes for a study of conducting additives in solid-state cathode composites.
Interplay of Cathode–Halide Solid Electrolyte in Enhancing Thermal Stability of Charged Cathode Material in All-Solid-State Batteries
ACS Energy Letters · 2024
Equipment · model
Ampoule Furnace · Model not specified
Annealing halide electrolytes for research on cathode–electrolyte thermal stability.